| Course Name | Code | Semester | T+U Hours | Credit | ECTS |
|---|---|---|---|---|---|
| Advanced Nmr Spectroscopy | KIM 583 | 0 | 3 + 0 | 3 | 6 |
| Precondition Courses | |
| Recommended Optional Courses | |
| Course Language | Turkish |
| Course Level | yuksek_lisans |
| Course Type | Optional |
| Course Coordinator | Prof.Dr. MUSTAFA ZENGİN |
| Course Lecturers | Prof.Dr. MUSTAFA ZENGİN, |
| Course Assistants | |
| Course Category | |
| Course Objective | Teaching of working principle of Nuclear Magnetic Resonance (NMR) spectroscopy, fields of application and interpretation of NMR spectra. |
| Course Content | Development of NMR Spectroscopy, Resonance Effect, chemical shift, Spin-spin interaction, Interactions Between Protons, Spin Systems, The slider Reagents and Double Resonance Effect, Dynamic NMR spectroscopy, 13C NMR Spectroscopy, Absorption and Resonance, Pulse NMR Spectroscopy, 13C NMR Chemical Shifts of Organic Compounds, Two-dimensional (2D)-NMR Spectroscopy |
| # | Course Learning Outcomes | Teaching Methods | Assessment Methods |
|---|---|---|---|
| 1 | Learning of the principle of NMR spectroscopy | Lecture, | Performance Task, |
| 2 | Learning of Resonance Event | Lecture, Question-Answer, Discussion, | Testing, Homework, |
| 3 | Learning of chemical shift | Lecture, Question-Answer, Discussion, | Testing, Homework, |
| 4 | Interpretation of 1H NMR, 13C NMR ve 2D-NMR spectroscopy | Lecture, Question-Answer, Discussion, Lab / Workshop, Self Study, | Testing, Homework, |
| Week | Course Topics | Preliminary Preparation |
|---|---|---|
| 1 | Development and Application Areas of NMR Spectroscopy | Page: 1-5 |
| 2 | Resonance Event | Page: 7-21 |
| 3 | Chemical Shift | Page: 25-81 |
| 4 | Spin-Spin Interaction | Page: 93-140 |
| 5 | Interactions Between Protons Spin Systems | Page: 141-54 |
| 6 | Spin Systems | Page: 165-194 |
| 7 | Slider Reagents and Double Resonance Event | Page: 207-213 |
| 8 | Dynamic NMR spectroscopy | Page: 221-226 |
| 9 | 13C NMR Spectroscopy | Page: 241-245 |
| 10 | Absorption and Resonance | Page: 249-259 |
| 11 | Pulse NMR Spectroscopy | Page: 263-296 |
| 12 | 13C NMR Chemical Shifts of Organic Compounds | Page: 311-341 |
| 13 | Two-dimensional (2D)-NMR Spectroscopy | Page: 401-431 |
| 14 | Example Solution of NMR spectra |
| Resources | |
|---|---|
| Course Notes | Balcı, M., Nükleer Manyetik Rezonans Spektroskopisi, ODTÜ Yayıncılık, 2011 |
| Course Resources | Webb, G.A., Nuclear Magnetic Resonance, Royal Society of Chemistry, 2009 |
| Order | Program Outcomes | Level of Contribution | |||||
|---|---|---|---|---|---|---|---|
| 1 | 2 | 3 | 4 | 5 | |||
| 1 | In addition to expanding and making deeper the knowledge established on undergraduate education in a same or different area, reaches the knowledge by doing research and also improves his or her knowledge to the expertise level by doing evaluation and practice. | X | |||||
| 2 | Utilizing incomplete or limited data in his or her study area expands the knowledge by experimental methods and use those obtained knowledge by scientific, social and ethical responsibility. | X | |||||
| 3 | - Constructs a problem with his/her adviser and develops a solution method and by evaluating the results apply them if it is necessary in his/ her area. | X | |||||
| 4 | -Transfer the current developments and his/her studies to the other related or nonrelated groups as written, orally and visually. | X | |||||
| 5 | - Develops new strategic approach and produces solutions in unexpected and complicated situations in his or her area of practice. | X | |||||
| 6 | - Develops strategic and practice plans and evaluates the obtained results within the framework of quality process in his or her study area. | X | |||||
| 7 | - Has written communication ability in one of well known foreign languages (“European Language Portfolio Global Scale”, Level A1). | X | |||||
| 8 | -Has knowledge for software and hardware about computers and uses data processing. | X | |||||
| 9 | Protecting scientific, social, and ethical values, teaches and controls these values in the steps of collection, evaluation and announcement of data in the international arena. | X | |||||
| 10 | - Applies his or her digested knowledge and problem solving ability in advanced studies. | X | |||||
| Evaluation System | |
|---|---|
| Semester Studies | Contribution Rate |
| 1. Ödev | 70 |
| 1. Performans Görevi (Seminer) | 30 |
| Total | 100 |
| 1. Yıl İçinin Başarıya | 50 |
| 1. Final | 50 |
| Total | 100 |
| ECTS - Workload Activity | Quantity | Time (Hours) | Total Workload (Hours) |
|---|---|---|---|
| Course Duration (Including the exam week: 16x Total course hours) | 16 | 3 | 48 |
| Hours for off-the-classroom study (Pre-study, practice) | 16 | 3 | 48 |
| Mid-terms | 1 | 15 | 15 |
| Assignment | 1 | 10 | 10 |
| Performance Task (Seminar) | 1 | 10 | 10 |
| Final examination | 1 | 20 | 20 |
| Total Workload | 151 | ||
| Total Workload / 25 (Hours) | 6.04 | ||
| dersAKTSKredisi | 6 | ||