Course Name Code Semester T+U Hours Credit ECTS
Synthesis Of Nano Particulates NMB 512 0 3 + 0 3 6
Precondition Courses None
Recommended Optional Courses
Course Language English
Course Level yuksek_lisans
Course Type Optional
Course Coordinator Prof.Dr. ALİ OSMAN KURT
Course Lecturers Prof.Dr. ALİ OSMAN KURT,
Course Assistants
Course Category Field Proper Education
Course Objective This course will be able to prepare postgraduate students in a way that they can define nanoparticulates, their properties, the way that nanoparticulates have been characterized, their production methods and hazards associated in their synthesis and uses.
Course Content Nanoparticulates: Nonopowders, shape factor, properties and characterizations. Synthesis of nanoparticulates; Physical Vapour Deposition (PVD) techniques such as IGC, CM, AD and HPMR. Chemical Vapour Deposition (CVD) techniques. Chemical Vapour Condensation (CVC) techniques (MPP, Combustion Flame Pyrolysis, Laser Pyrolysis). Conventional Spray Pyrolysis (Electrospray, Low-pressure spray pyrolysis, Salt-assisted spray pyrolysis, Ultrasonic spray pyrolysis). Chemical synthesis in solution. Mechanical alloying. Hazards associated synthesis and using them.
# Course Learning Outcomes Teaching Methods Assessment Methods
1 to define nanoparticulates in terms of shape, properties and characterizations. Lecture, Question-Answer, Discussion, Testing, Oral Exam, Homework,
2 to explain and to write syntesis of nanoparticulates using mechanical methods. Lecture, Question-Answer, Discussion, Testing, Oral Exam, Homework,
3 to explain and to write syntesis of nanoparticulates using chemical methods Lecture, Question-Answer, Discussion, Testing, Oral Exam, Homework,
4 to explain and to write syntesis of nanoparticulates using pyrolysis techniques. Lecture, Question-Answer, Discussion, Testing, Oral Exam, Homework,
5 to explain and to write what hazards associated in synthesising and using nanoparticulates. Lecture, Question-Answer, Discussion, Testing, Oral Exam, Homework,
Week Course Topics Preliminary Preparation
1 Introduction: Nanoparticulate, nanopowder, terms, applications.
2 Nanopartuculate ? shape factor, properties and defining them.
3 Hazards associated in synthesising and using them.
4 Synthesis of nanoparticulates: general approch and special techniques.
5 Chemical vapour deposition: Thermally-activated Chemical Vapour Deposition (CVD), Plasma-Enhanced Chemical Vapour Deposition.
6 Chemical vapour deposition: Laser-Assisted Chemical Vapour Deposition.
7 Chemical vapour condensation: Thermally Activated Chemical Vapour Condensation (CVC), Microwave Plasma Process (MPP).
8 Chemical vapour condensation: Combustion Flame Pyrolysis, Laser Pyrolysis.
9 Synthesis of nanoparticulates: Physical vapour deposition: Physical Vapour Deposition (PVD), Inert Gas Condensation (IGC), Cryogenic Melting (CM), Arc Discharge (AD), Hydrogen Plasma Melting Reaction (HPMR).
10 Synthesis of nanoparticulates: Spray pyrolysis: Conventional Spray Pyrolysis, Electrospray, Low-pressure spray pyrolysis.
11 Synthesis of nanoparticulates: Spray pyrolysis: Salt-assisted spray pyrolysis, Ultrasonic spray pyrolysis.
12 Synthesis of nanoparticulates: Chemical synthesis in solution: Growth in microemulsions, Growth in presence of surface stabilising agents, Conventional Hydro thermal methods.
13 Synthesis of nanoparticulates: Chemical synthesis in solution: Hydrothermal synthesis in supercritical solvents, Sol-gel methods, Sonochemical methods, Electrodeposition methods.
14 Synthesis of nanoparticulates: With mechanical alloying.
Resources
Course Notes
Course Resources 1. Powders and bulk solids : behavior, characterization, storage and flow Schulze, Dietmar, ISBN-ISSN: 9783540737674, New York : Springer , 2008.
2. Nanostructures & Nanomaterials : Synthesis, Properties & Applications Cao, Guozhong, ISBN-ISSN: 1860944809 London, 2007.
3. Nanomaterials: synthesis, properties, and applications, edited by A.S. Edelstein and R.C. Cammarata. ISBN-ISSN: 0750305789, Philadelphia, 1996.
4. Nanopowders and nanocoatings: production, properties and applications V.F. Cotler, editor. ISBN-ISSN: 9781617618079 New York: Nova Science Publishers, 2010.
Order Program Outcomes Level of Contribution
1 2 3 4 5
1 X
2
3 X
4 X
5 X
6
7 X
8
9
10
11 X
12
Evaluation System
Semester Studies Contribution Rate
1. Ara Sınav 40
1. Ödev 20
2. Ödev 20
1. Performans Görevi (Seminer) 20
Total 100
1. Yıl İçinin Başarıya 60
1. Final 40
Total 100
ECTS - Workload Activity Quantity Time (Hours) Total Workload (Hours)
Course Duration (Including the exam week: 16x Total course hours) 16 3 48
Hours for off-the-classroom study (Pre-study, practice) 16 3 48
Mid-terms 1 13 13
Quiz 1 2 2
Assignment 1 20 20
Oral Examination 1 10 10
Final examination 1 10 10
Total Workload 151
Total Workload / 25 (Hours) 6.04
dersAKTSKredisi 6